Analytical chemistry is the rapidly progressing branch of chemistry, which deals with the study of analytical tools with matter. Thus, the novel techniques emerging in analytical chemistry are facilitating quick and reliable measurement. The primary objective of book entitled Fundamental of analytical chemistry is to provide fundamental knowledge of the analytical principles. The massive scope of the subject dictates the all-possible visual assistance is avoidable to the students. This has done by presenting a large no of questions and examples serve to reinforce as well as assist the students to learning the subject. The present edition designed to use as a textbook as well as competitive book by the students of B.Sc. and M.Sc. It is also serve as a reference manual for practisiging ananlytical chemists and research students.